Electrochemical Determination of Sesamol in Foods by Square Wave Voltammetry at a Boron-Doped Diamond Electrode


ASLIŞEN B., KOÇAK Ç. C., KOÇAK S.

Analytical Letters, vol.53, no.3, pp.343-354, 2020 (SCI-Expanded, Scopus) identifier

  • Publication Type: Article / Article
  • Volume: 53 Issue: 3
  • Publication Date: 2020
  • Doi Number: 10.1080/00032719.2019.1650752
  • Journal Name: Analytical Letters
  • Journal Indexes: Science Citation Index Expanded (SCI-EXPANDED), Scopus, Academic Search Premier, Aerospace Database, Aquatic Science & Fisheries Abstracts (ASFA), BIOSIS, Biotechnology Research Abstracts, CAB Abstracts, Chimica, Communication Abstracts, Food Science & Technology Abstracts, Metadex, Veterinary Science Database, Civil Engineering Abstracts
  • Page Numbers: pp.343-354
  • Keywords: Boron-doped diamond electrode (BDDE), cyclic voltammetry (CV), sesamol, square wave voltammetry (SWV), tahini halva
  • Manisa Celal Bayar University Affiliated: Yes

Abstract

Sesamol is a phenolic compound naturally found in sesame seeds. It has beneficial health effects in humans, as it features significant antioxidant activity and has anticancer and anti-aging properties. Therefore, finding a suitable electrode surface for sesamol determination is important. The prominent advantage of boron-doped diamond electrodes is their use in many sensing platforms without the need for the surface modification. This study represents the first time that sesamol has been determined using boron-doped diamond electrodes in acidic media by square wave voltammetry. Linear responses of sesamol were obtained in the concentration range from 0.2 µM to 1000 µM, and the detection limit was determined to be 85 nM based on a signal-to-noise ratio of 3. The relative standard deviations were 2.1% for a 1 µM standard with three measurements.